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The ability to produce, synthesize and manufacture large quantities of 5-Bromo-1-indanone (34598-49-7) with quality control system under CGMP manufacturing
5-Bromo-1-indanone is a starting compound for indanone-based pharmaceuticals. At the same time, it is also the raw material used in the synthesis. The application is an useful organic synthesis building block. Its synonym are：
5-BROMOINDAN-1-ONE;5-BROMOINDANONE;5-BROMO-1-INDANONE;1-Indanone, 5-bromo-;5-Bromo-1-indanone,98%;5-Bromo-1-indanone 98%.
Bromination of 4-bromoindanone and 5-bromoindanone, facile synthetic access to 3,5,10-tribromo-7H-benzo[c]fluoren-7-one. Bromination reactions of 5-bromoindanone were presented in the experiment and its optimum reaction conditions. 2,2,4-Tribromoindanone was synthesized by treatment of 4-bromoindanone with molecular bromine at room temperature in a high yield. Bromination of 4-bromoindanone with NBS, SiO2 and LiClO4 in PEG yielded the corresponding 2,4-dibromoindanone which was reduced to 1-hydroxy-2,4-dibromoindane. Acetylation of hydroxydibromoindane in pyridine gave the 1-acetoxy-2,4-dibromoindane in excellent yield. The radical bromination of 5-bromoindanone with NBS at 77°C in CCl4 yielded the corresponding 3,5-dibromoindene-1-one which was converted to 3,5,10-tribromo-7H-benzo[c]fluoren-7-one by thermolysis.
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5-Bromo-1-indanone (34598-49-7) Specifications
|CAS Min %||97.5|
|CAS Max %||100.0|
|Chemical Name or Material||5-Bromo-1-indanone|
|Molecular Weight (g/mol)||211.058|
|Color||Beige through Brown|
|Melting Point||126.0° to 130.0°C|
5-Bromo-1-indanone (34598-49-7) Safety and Handling
(34598-49-7) GHS H Statement
- Causes skin irritation.
- Causes serious eye irritation.
- Harmful if swallowed.
- May cause respiratory irritation.
5-Bromo-1-indanone GHS P Statement:
- Avoid breathing dust/fume/gas/mist/vapors/spray.
- IF SWALLOWED: Call a POISON CENTER or doctor/physician if you feel unwell.
- IF ON SKIN: Wash with plenty of soap and water.Wear protective gloves/protective clothing/eye protection/face protection.
- IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
WARNING: The information provided on this web site was developed in compliance with European Union (EU) regulations and is correct to the best of our knowledge, information and belief at the date of its publication. The information given is designed only as a guide for safe handling and use. It is not to be considered as either a warranty or quality specification.315-H319-H335.
5-Bromo-1-indanone (34598-49-7) Articles
Bromination of 4-bromoindanone and 5-bromoindanone, facile synthetic access to 3,5,10-tribromo-7H-benzo[c]fluoren-7-one
Bromination reactions of 5-bromoindanone were presented in the experiment and its optimum reaction conditions. ….
Journal of the Chemical Society of Pakistan 2016 vol. 38 # 3 p. 546 – 552
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